COMPOST MANURE TESTING METHODS
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Moisture/Dry Matter
105-110 degrees Celsius for 16 hours Method 2.0 from “Recommended Methods of Manure Analysis” Method 2.2
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Total Nitrogen
Combustion by Elementar Vario Max CN Method 3.3 from “Recommended Methods of Manure Analysis” and TMECC method 4.02 (adapted from AOAC 990.03)
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Total Carbon
Combustion by Elementar Vario Max CN Method 4.01 from the “Test Methods for the Examination of Composting and Compost” (TMECC)
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Ammonium-N
KCL Extraction determined on FIA Lab flow injection autoanalyzer. Method 4.3 from “Recommended Methods of Manure Analysis” (Adapted from USEPA 350.1)
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Nitrate-N
KCL Extraction determined on FIA Lab flow injection autoanalyzer. (Adapted from USEPA 353.2)
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Mineral Digestion
Nitric acid digestion in CEM Mars Microwave system. Method 5.3 from “Recommended Methods of Manure Analysis” and TMECC 4.12 (Adapted from EPA 3051) use for determination of P,K,Ca,Mg,Na,B,Co,Cu,Zn,Mo,Mn,Fe,S,Al
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Mineral Determination
The digested samples are analyzed on Thermal 6500 Dou ICP. Method 6.3 from “Recommended Methods of Manure Analysis” and TMECC 4.14
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pH
Liquid samples are done as-is. Solid samples are analyzed one part sample to 2 parts water. Method 7 from “Recommended Methods of Manure Analysis”
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Conductivity (EC)
Liquid samples are done as-is. Solid samples are analyzed one part sample to 2 parts water. Method 8 from “Recommended Methods of Manure Analysis”
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Water Extractable Phosphorus
100:1 solution:solids ratio, sample is shaken for one hour at 150 rpm. Sample is then filtered and analyzed on ICP (Reference Wolf, Ann, Peter Kleinman, Andrew Sharpley et.al. Soil Sci.Soc.Am.J
66:2009-2015
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Organic Matter/Ash
Samples muffled in an ashing oven at 550 degrees Celsius for 2 hours. Method 5.07 from the TMECC (EPA method 160.4)
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Maturity
Solvita Maturity Test (Method 5.08E from “Test Methods for the Examination of Composting and Compost”)
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Inert Materials
Method 3.08 from “Test Methods for the Examination of Composting and Compost”